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Study of the Structural, Morphological, and Electrical Properties of Pyrrole/Activated Carbon Derived from Rice Husk on Cotton Fabric | ||
| Progress in Physics of Applied Materials | ||
| دوره 6، شماره 4 - شماره پیاپی 13، اسفند 2026، صفحه 305-313 اصل مقاله (1.29 M) | ||
| نوع مقاله: Original Article | ||
| شناسه دیجیتال (DOI): 10.22075/ppam.2026.40057.1192 | ||
| نویسندگان | ||
| Manash Jyoti Das1؛ Mohd Zaki Mohd Yusoff* 1، 2؛ Suraya Ahmad Kamil1؛ Ali H. Jawad3، 4، 5؛ Muhammad Syarifuddin Yahya6؛ Syahril Amin Hashim7 | ||
| 1School of Physics and Material Studies, Faculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia | ||
| 2Institute for Biodiversity and Sustainable Development (IBSD), Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia | ||
| 3Advanced Biomaterials and Carbon Development (ABCD) Research Group, Faculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia | ||
| 4Environmental and Atmospheric Sciences Research Group, Scientific Research Center, Al-Ayen University, Thi-Qar, Nasiriyah, 64001, Iraq | ||
| 5UNESCO RCQE Chair in Emerging Renewable & Sustainable Energy Technologies, Sohar University, PO Box 44, PCI 311, Sohar – Oman | ||
| 6Energy Storage Research Group, Faculty of Ocean Engineering Technology and Informatics, Universiti Malaysia Terengganu, 21030 Kuala Nerus, Terengganu, Malaysia | ||
| 7Material Characterisation Lab, Centralised Lab Management Centre, Universiti Sultan Zainal Abidin, Gong Badak Campus, 21300 Kuala Terengganu, Terengganu, Malaysia. | ||
| تاریخ دریافت: 24 آذر 1404، تاریخ بازنگری: 23 اردیبهشت 1405، تاریخ پذیرش: 25 اردیبهشت 1405 | ||
| چکیده | ||
| In this work, activated carbon (AC) and pyrrole were successfully deposited onto cotton fabric using simple dip and dry methods. First, the fabric was bleached. Next, a mixture of AC derived from rice husk, polyvinyl alcohol (PVA) as a binding agent, and sodium dodecylbenzene sulphonate (SDBS) as a surfactant was prepared. This mixture was applied to the fabric using a brush. After that, the AC treated fabric was submerged in a pyrrole solution of the desired molarity, followed by immersion in a ferric chloride (FeCl₃) solution for 2 h. Four samples were prepared, and structural, morphological, and electrical characterisation was performed using field emission scanning electron microscopy (FESEM), energy dispersive X ray spectroscopy (EDX), and Fourier transform infrared (FTIR) spectroscopy. Electrical characterisation was conducted using a four point probe method at room temperature for 2 min on 1 × 1 cm² samples. Among all the samples, PPy/AC/cotton fabric (2) exhibited the highest conductivity of 5.5 S/cm. The study also demonstrated that increasing the molarity of pyrrole and FeCl₃ initially enhanced the conductivity. However, when the molarities were increased to 0.3 M pyrrole and 0.6 M FeCl₃, as well as 0.4 M pyrrole and 0.8 M FeCl₃, the conductivity decreased, and the fabric became stiffer and more rigid. | ||
| کلیدواژهها | ||
| Activated carbon؛ Pyrrole؛ PVA؛ SDBS؛ Molarity | ||
| مراجع | ||
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[1] Li, Q.L., Zhang, C.R., Xue, Z.S. and Li, J.Q., 2010. Preparation and characterization of polypyrrole microbelt via cotton template. Chinese Journal of Chemical Physics, 23(2), pp.207-210.
[2] Yaghoubidoust, F., Wicaksono, D.H., Chandren, S. and Nur, H., 2014. Effect of graphene oxide on the structural and electrochemical behavior of polypyrrole deposited on cotton fabric. Journal of Molecular Structure, 1075, pp.486-493.
[3] Tat’yana, V.V. and Efimov, O.N., 1997. Polypyrrole: a conducting polymer; its synthesis, properties and applications. Russian Chemical Reviews, 66(5), pp.443-457.
[4] Thakur, A.K., Choudhary, R.B., Majumder, M. and Gupta, G., 2017. In-situ integration of waste coconut shell derived activated carbon/polypyrrole/rare earth metal oxide (Eu2O3): a novel step towards ultrahigh volumetric capacitance. Electrochimica Acta, 251, pp.532-545.
[5] Daffalla, S.B., Mukhtar, H. and Shaharun, M.S., 2012. Properties of activated carbon prepared from rice husk with chemical activation. International Journal of Global Environmental Issues, 12(2-4), pp.107-129.
[6] Islam, R., Khair, N., Ahmed, D.M. and Shahariar, H., 2019. Fabrication of low cost and scalable carbon-based conductive ink for E-textile applications. Materials Today Communications, 19, pp.32-38.
[7] Wang, Y., Kong, Q., Liu, Q., Li, R., Zhou, C. and Li, Z., 2024. Preparation of polypyrrole/carbon nanotubes composite cotton fabric through in situ polymerization and its conductive property. ACS Applied Electronic Materials, 6(5), pp.3563-3573.
[8] Liu, C., Cai, Z., Zhao, Y., Zhao, H. and Ge, F., 2016. Potentiostatically synthesized flexible polypyrrole/multi-wall carbon nanotube/cotton fabric electrodes for supercapacitors. Cellulose, 23(1), pp.637-648.
[9] Lima, R.M., Alcaraz-Espinoza, J.J., da Silva Jr, F.A. and de Oliveira, H.P., 2018. Multifunctional wearable electronic textiles using cotton fibers with polypyrrole and carbon nanotubes. ACS Applied Materials & Interfaces, 10(16), pp.13783-13795.
[10] Cetiner, S., 2014. Dielectric and morphological studies of nanostructured polypyrrole-coated cotton fabrics. Textile Research Journal, 84(14), pp.1463-1475.
[11] Milanović, J., Kostić, M. and Škundrić, P., 2012. Structure and properties of tempo-oxidized cotton fibers. Chemical Industry & Chemical Engineering Quarterly, 18(3), pp.473-481.
[12] Varesano, A., Aluigi, A., Florio, L. and Fabris, R., 2009. Multifunctional cotton fabrics. Synthetic Metals, 159(11), pp.1082-1089.
[13] Muniandy, L., Adam, F., Mohamed, A.R. and Ng, E.P., 2014. The synthesis and characterization of high purity mixed microporous/mesoporous activated carbon from rice husk using chemical activation with NaOH and KOH. Microporous and Mesoporous Materials, 197, pp.316-323.
[14] Khadem, F., Pishvaei, M., Salami‐Kalajahi, M. and Najafi, F., 2017. Morphology control of conducting polypyrrole nanostructures via operational conditions in the emulsion polymerization. Journal of Applied Polymer Science, 134(15).
[15] Shanmugapriya, C. and Velraj, G., 2012. FT-IR spectroscopy and SEM-EDX studies on nano copper doped conducting polymer. Advanced Materials Research, 584, pp.541-545.
[16] Vinitha, M. and Velraj, G., 2022. Synthesis and characteristic studies on pure and nano silver oxide-doped polypyrrole for supercapacitor application. Journal of Materials Science: Materials in Electronics, 33(9), pp.6627-6635.
[17] Syamimi, N. and Yahud, S., 2021. Electrical characterisation of polypyrrole thin film conducting polymer. Journal of Physics: Conference Series, 2129(1), p.012051. | ||
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