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Synthesis and characterization of undoped and Fe–doped SnO2 nanoparticles | ||
Innovations in Materials: Current & Future | ||
مقالات آماده انتشار، پذیرفته شده، انتشار آنلاین از تاریخ 19 آبان 1393 | ||
نوع مقاله: Original Paper | ||
شناسه دیجیتال (DOI): 10.22075/ancr.2014.217 | ||
نویسنده | ||
Mousa Aliahmad* | ||
University of Sistan and Baluchestan | ||
تاریخ دریافت: 22 خرداد 1393، تاریخ بازنگری: 04 آبان 1393، تاریخ پذیرش: 19 آبان 1393 | ||
چکیده | ||
A B S T R A C T Tin oxide (SnO2) nanoparticles have been successfully prepared by using co-precipitation route using tin chloride and sodium hydroxide as tin source and precipitating agent, respectively. Fourier transform infrared spectrum, x-ray powder diffraction, scanning electron microscope, energy dispersive x-ray spectroscopy and transmission electron microscope were used to characterize as-prepared and heated samples. The broad XRD peaks were corresponding to small crystallite nanoparticles. Grain size of particles has been obtained around 6 nanometers using XRD patterns and Scherer’s formula. SEM images were shown rod morphology of nanoparticles and also one can see a good monodispirsity of rods. The particle size was obtained less than 20 nm using TEM images. Nice superparamagnetic property was obtained when the samples calcinated at 200 °C. The particle size decreased as doping amount increasing. PACS Nos: 75.75.-c | ||
کلیدواژهها | ||
Tin dioxide؛ co-precipitation؛ nanoparticles and rods | ||
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