Synthesis, characterization and investigation of catalytic properties of NiCo2O4@Ni(BDC) metal-organic framework in the preparation of chromeno[2,3-b]pyridine derivatives | ||
| شیمى کاربردى روز | ||
| Article 7, Volume 15, Issue 56, September 2020, Pages 101-116 PDF (676.04 K) | ||
| Document Type: Original Article | ||
| DOI: 10.22075/chem.2020.18185.1666 | ||
| Authors | ||
| Mohammad Ali Ghasemzadeh* 1; Boshra Mirhosseini-Eshkevari2; Manzarbanoo Esnaashari3 | ||
| 1Department of Chemistry, Qom Branch, Islamic Azad University, Qom, P.O. Box 37491-13191. R. Iran | ||
| 2Department of Chemistry, Qom Branch, Islamic Azad University, Qom, I. R. Iran | ||
| 3Department of Chemistry, North Tehran Branch, Islamic Azad University, Tehran, I. R. Iran | ||
| Receive Date: 03 July 2019, Revise Date: 01 November 2019, Accept Date: 01 January 2020 | ||
| Abstract | ||
| Metal-organic frameworks have attracted considerable attention because of their unique properties and potential applications in diverse fields. In this research, an efficient and simple method has been reported for the preparation of chromeno[2,3-b]pyridine derivatives through the multi-component reactions of salicylaldehydes, thiols and malononitrile in the presence of NiCo2O4@Ni(BDC) nanocatalyst. In this approache, the products were obtained in short reaction times and excellent yields. Moreover, the synthesized compounds were characterized by IR, 1HNMR and 13CNMR spectroscopy analysis. Also, the catalyst was fully characterized by spectroscopic techniques including field-emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), fourier transform infrared spectrophotometry (FT-IR), X-ray diffraction (XRD) analysis, transmission electron microscopy (TEM) and thermogravimetric analysis (TGA). | ||
| Keywords | ||
| Multi-Component Reactions; chromeno[2; 3-b]pyridine; Metal-Organic Frameworks; Ultrasound Irradiation; NiCo2O4@Ni(BDC) | ||
| References | ||
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