پیوندهای مفید
آمار
| تعداد نشریات | 21 |
| تعداد شمارهها | 702 |
| تعداد مقالات | 10,131 |
| تعداد مشاهده مقاله | 71,399,300 |
| تعداد دریافت فایل اصل مقاله | 63,119,037 |
Exploring the Effects of pH on the Morphology and Optical Characteristics of ZnFe2O4 Nanoparticles | ||
| Progress in Physics of Applied Materials | ||
| مقاله 8، دوره 5، شماره 1 - شماره پیاپی 8، مرداد 2025، صفحه 53-59 اصل مقاله (933.97 K) | ||
| نوع مقاله: Original Article | ||
| شناسه دیجیتال (DOI): 10.22075/ppam.2025.36655.1129 | ||
| نویسندگان | ||
| Mahdiyeh Taherkhani1؛ Mohammad Hossein Ehsani* 2؛ Reza Zarei moghadam3؛ Abbas Javadian4 | ||
| 1Thin Film Lab, Faculty of Physics, University of Semnan, Semnan, Islamic Republic of Iran | ||
| 2Faculty of Physics | ||
| 3Physics Department, Faculty of Science, Arak University, Arak, 38156, Iran | ||
| 4Physics | ||
| تاریخ دریافت: 01 بهمن 1403، تاریخ بازنگری: 17 بهمن 1403، تاریخ پذیرش: 23 بهمن 1403 | ||
| چکیده | ||
| In this paper, ZnFe2O4 nanoparticles were synthesized using the co-precipitation method, aiming to investigate the effect of pH on their structural and optical properties. The synthesis was carried out at various pH levels of 7, 9, and 11, to explore how acidic and basic conditions can influence the characteristics of these nanoparticles. Structural analysis was conducted using X-ray diffraction (XRD), which allowed for a comprehensive understanding of the phase composition and crystallinity of the nanoparticles. The XRD results revealed that as the pH increased from 7 to 11, the diffraction peaks became broader, indicating a reduction in crystalline size, which is a common phenomenon attributed to increased defects within the crystalline structure. This size reduction corresponds with an increase in dislocation density and strain within the samples, suggesting that higher pH environments lead to more significant structural alterations. Optical properties were investigated using a UV-Vis spectrometer. The optical analysis showed a noteworthy trend: as the pH increased from 7 to 11, the absorption capacity of the ZnFe2O4 nanoparticles decreased. This reduction in absorption may imply a modification in band gap energy, which is crucial for potential applications in photonic devices and sensors. | ||
| کلیدواژهها | ||
| ZnF2O4 Nanoparticles؛ Co-Precipitation Method؛ X-Ray Diffraction Pattern | ||
| مراجع | ||
|
[1] Korkmaz, A.D., Güner, S., Slimani, Y., Gungunes, H., Amir, M., Manikandan, A. and Baykal, A., 2019. Microstructural, optical, and magnetic properties of vanadium-substituted nickel spinel nanoferrites. Journal of Superconductivity and Novel Magnetism, 32, pp.1057-1065.
[2] Sharma, S., Kumar, D., Kumar, S., Goyat, M.S. and Mandal, P., 2018. Structural and optical properties of Cu incorporated ZnFe2O4 ferrite nanoparticles prepared by wet chemical route. Materials Chemistry and Physics, 212, pp.292-297.
[3] Nanda, D., Kumar, P. and Prakash, C., 2017. Synthesis and characterization of Ni-Cu-Zn ferrites by microwave reactive sintering technique. Integrated Ferroelectrics, 185(1), pp.183-192.
[4] Goya, G.F., Grazu, V. and Ibarra, M.R., 2008. Magnetic nanoparticles for cancer therapy. Current nanoscience, 4(1), pp.1-16.
[5] Sonia, L.C., Victory, M. and Phanjoubam, S., 2020. A comparative study of the properties of zinc ferrite nanoparticles synthesized by different techniques for nanofluid preparation. Integrated Ferroelectrics, 204(1), pp.100-111.
[6] Suppuraj, P., Thirunarayanan, G., Swaminathan, M. and Muthuvel, I., 2017. Facile synthesis of spinel nanocrystalline ZnFe2O4: enhanced photocatalytic and microbial applications. Mater Sci Appl Chem, 34(1), pp.5-11.
[7] Vinosha, P.A., Mely, L.A., Jeronsia, J.E., Krishnan, S. and Das, S.J., 2017. Synthesis and properties of spinel ZnFe2O4 nanoparticles by facile co-precipitation route. Optik, 134, pp.99-108.
[8] Iqbal, F., Abd Mutalib, M.I., Shaharun, M.S. and Abdullah, B., 2016. Synthesis of ZnFe2O4 using sol-gel method: effect of different calcination parameters. Procedia engineering, 148, pp.787-794.
[9] Liu, R., Lv, M., Wang, Q., Li, H., Guo, P. and Zhao, X.S., 2017. Solvothermal synthesis of size-tunable ZnFe2O4 colloidal nanocrystal assemblies and their electrocatalytic activity towards hydrogen peroxide. Journal of Magnetism and Magnetic Materials, 424, pp.155-160.
[10] Sun, Hao, He Cai, Linli Li, Yuan Yang, Pan He, Kun Zhou, Yu Han, Jie Guan, and Xiaoxing Fan. "Photothermal synergic catalytic degradation of the gaseous organic pollutant isopropanol in oxygen vacancies utilizing ZnFe2O4." Journal of Chemical Research 45 (9) 773-780 (2021).
[11] Ashrafi, M. Molla Ali, H. Rezagholipour Dizaji, M. H. Ehsani, and R. Zarei Moghadam. "ZnS Film properties modification using oblique angle deposition technique." Surface Review and Letters 25, no. 06 1850119 (2018).
[12] Moghadam, R.Z., Dizaji, H.R., Ehsani, M.H., Kameli, P. and Jannesari, M., 2019. Correlation study of structural, optical, and hydrophobicity properties of diamond-like carbon films prepared by an anode layer source. Materials Research Express, 6(5), p.055601.
[13] Surendra, B.S., Nagaswarupa, H.P., Hemashree, M.U. and Khanum, J., 2020. Jatropha extract mediated synthesis of ZnFe2O4 nanopowder: Excellent performance as an electrochemical sensor, UV photocatalyst and an antibacterial activity. Chemical Physics Letters, 739, p.136980.
[14] Moghadam, R.Z., Dizagi, H.R., Agren, H. and Ehsani, M.H., 2023. Understanding the effect of Mn2+ on Yb3+/Er3+ co-doped NaYF4 upconversion and obtaining the optimal combination of these tridoping. Scientific Reports, 13(1), p.17556.
[15] Moghadam, R.Z., Dizaji, H.R., Ehsani, M.H., Kameli, P. and Jannesari, M., 2019. Correlation study of structural, optical, and hydrophobicity properties of diamond-like carbon films prepared by an anode layer source. Materials Research Express, 6(5), p.055601.
[16] Surendra, B.S., Nagaswarupa, H.P., Hemashree, M.U. and Khanum, J., 2020. Jatropha extract mediated synthesis of ZnFe2O4 nanopowder: Excellent performance as an electrochemical sensor, UV photocatalyst and an antibacterial activity. Chemical Physics Letters, 739, p.136980.
[17] Manohar, A., Vijayakanth, V. and Kim, K.H., 2021. Influence of Ca doping on ZnFe2O4 nanoparticles magnetic hyperthermia and cytotoxicity study. Journal of Alloys and Compounds, 886, p.161276.
[18] Ahmed, A., Niazi, M.B.K., Jahan, Z., Ahmad, T., Hussain, A., Pervaiz, E., Janjua, H.A. and Hussain, Z., 2020. In-vitro and in-vivo study of superabsorbent PVA/Starch/g-C3N4/Ag@ TiO2 NPs hydrogel membranes for wound dressing. European Polymer Journal, 130, p.109650.
[19] Alhusaiki-Alghamdi, H.M., 2024. Structural, Optical, Electrical, and Magnetic Characterization of PC/PEO Blend Incorporated with ZnFe2O4 Nanoparticles. Advances in Polymer Technology, 9443289 (2024).
[20] Li, Z.M., Wei, Z.Q., Ding, M.J., Yu, Q.S., Zhu, J., Bai, J.L. and Zhang, H.N., 2025. Photoelectrochemical and optical fenton properties of Cu-doped ZnFe2O4 composites synthesized by hydrothermal method. Journal of Materials Science: Materials in Electronics, 36(2), pp.1-13.
| ||
|
آمار تعداد مشاهده مقاله: 868 تعداد دریافت فایل اصل مقاله: 485 |
||