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Synthesis and characterization of undoped and Fe–doped SnO2 nanoparticles | ||
| Innovations in Materials: Current & Future | ||
| مقاله 7، دوره 2.، شماره 1، فروردین 2015 اصل مقاله (2.23 M) | ||
| نوع مقاله: Original Paper | ||
| شناسه دیجیتال (DOI): 10.22075/ancr.2014.217 | ||
| نویسنده | ||
| Mousa Aliahmad* | ||
| University of Sistan and Baluchestan | ||
| تاریخ دریافت: 22 خرداد 1393، تاریخ بازنگری: 04 آبان 1393، تاریخ پذیرش: 19 آبان 1393 | ||
| چکیده | ||
| Tin oxide (SnO2) nanoparticles have been successfully prepared using co-precipitation route using of tin chloride and sodium hydroxide as tin source and precipitating agent, respectively. Fourier transform infrared spectrum, x-ray powder diffraction, scanning electron microscope, energy dispersive x-ray spectroscopy and transmission electron microscope were used to characterize as-prepared and heated samples. The broad XRD peaks were corresponding to small crystallitenanoparticles. Grain size of particles has been obtained around 6 nanometers using XRD patterns and Scherer’s formula. SEM images were shown as rod morphology of nanoparticles and also a good monodispirsity of rods could be seen. The particle size was obtained less than 20 nm using TEM images. Nice superparamagneticproperty was obtained when the samples were calcinated at 200 °C. The particle size decreased as doping amount increased. | ||
| کلیدواژهها | ||
| Tin dioxide؛ co-precipitation؛ nanoparticles and rods | ||
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