Khan, Naghma, Vijayan, N., Kumar, Ravinder, Gupta, Neha, Pant, R.P.. (1402). Preparation of Indian Reference Material for the calibration of Powder X-ray Diffractometer: α-Alumina. هنرهای کاربردی, 3(1), 57-65. doi: 10.22075/ppam.2023.31242.1059
Naghma Khan; N. Vijayan; Ravinder Kumar; Neha Gupta; R.P. Pant. "Preparation of Indian Reference Material for the calibration of Powder X-ray Diffractometer: α-Alumina". هنرهای کاربردی, 3, 1, 1402, 57-65. doi: 10.22075/ppam.2023.31242.1059
Khan, Naghma, Vijayan, N., Kumar, Ravinder, Gupta, Neha, Pant, R.P.. (1402). 'Preparation of Indian Reference Material for the calibration of Powder X-ray Diffractometer: α-Alumina', هنرهای کاربردی, 3(1), pp. 57-65. doi: 10.22075/ppam.2023.31242.1059
Khan, Naghma, Vijayan, N., Kumar, Ravinder, Gupta, Neha, Pant, R.P.. Preparation of Indian Reference Material for the calibration of Powder X-ray Diffractometer: α-Alumina. هنرهای کاربردی, 1402; 3(1): 57-65. doi: 10.22075/ppam.2023.31242.1059

Preparation of Indian Reference Material for the calibration of Powder X-ray Diffractometer: α-Alumina

Progress in Physics of Applied Materials
دوره 3، شماره 1 - شماره پیاپی 4، بهمن 2023، صفحه 57-65    اصل مقاله (871.5 K)
نوع مقاله: Original Article
شناسه دیجیتال (DOI): 10.22075/ppam.2023.31242.1059
نویسندگان
Naghma Khan1، 2؛ N. Vijayan* 1، 2؛ Ravinder Kumar1، 3؛ Neha Gupta4؛ R.P. Pant2
1Academy of Scientific and Innovative Research (AcSIR), Ghaziabad- 201 002, India
2CSIR-National Physical Laboratory, Dr. K.S. Krishnan Road, New Delhi – 110 012, India
3Central Research Facility, Indian Institute of Technology Delhi, Hauz Khas, New Delhi 110016, India
4Lajpat Rai College, Sahibabad, Ghaziabad -Uttar Pradesh- 201005, India
چکیده
The CSIR- National Physical Laboratory of India (NPLI) constantly prepares and disseminates Indian Reference Materials (Bharatiya Nirdeshak Dravya; BND®) in various areas. Recently, NPLI has prepared the Indian Reference Material (IRM) of α-Alumina to calibrate the Powder X-Ray Diffractometer (PXRD). In this report, the preparation and certification procedure of α-Alumina (BND 2001) has been examined as an Indian Reference Material that can be utilized as the primary standard for powder X-ray diffraction instruments. The developed IRM was utilized to calibrate PXRD for phase purity. The stability of the prepared α-alumina was studied by using powder X-ray diffractometer. The homogeneity and the particle size of the material were characterized by using scanning electron microscopy. The repeatability of the preparation and pertinent characterization were affirmed using different calibrated instruments. The phase purity of the material was verified by performing a round-robin test, and the related uncertainty estimations were reported in the paper.
کلیدواژه‌ها
Bharatiya Nirdeshak Dravya (BND®)؛ powder X-Ray diffraction؛ intensity calibration؛ uncertainty calculation؛ certification
مراجع
آمار
تعداد مشاهده مقاله: 565
تعداد دریافت فایل اصل مقاله: 630
دانشگاه سمنان
پیوندهای مفید
آمار
تعداد نشریات22
تعداد شماره‌ها722
تعداد مقالات10,383
تعداد مشاهده مقاله72,838,966
تعداد دریافت فایل اصل مقاله64,535,575