One-pot and three-component of tetrahydrobenzo [b] pyran derivatives using heterogeneous and recyclable catalysts and its application toward silver nanoparticle synthesis | ||
| شیمى کاربردى روز | ||
| Article 15, Volume 13, Issue 48, September 2018, Pages 209-230 PDF (1.3 M) | ||
| Document Type: Original Article | ||
| DOI: 10.22075/chem.2018.11772.1143 | ||
| Authors | ||
| Behrooz Maleki* ; sedigheh ayazi Jannat Abadi1; Mehdi Baghayeri1; Hossein Asghar Rahnamaye Aliabad2; Hojat Veisi3 | ||
| 1Department of Chemistry, Hakim Sabzevari University, Sabzevar, 96179-76487, Iran | ||
| 2Department of Physics, Hakim Sabzevari University, Sabzevar, Iran | ||
| 3Department of Chemistry, Payame Noor University, Tehran, Iran | ||
| Receive Date: 01 July 2017, Revise Date: 05 October 2017, Accept Date: 28 April 2018 | ||
| Abstract | ||
| An efficient, simple and green procedure has been developed for the synthesis of tetrahydrobenzo[b]pyran deravitives via the condensation one-pot and three-component of aldehydes, malononitrile and 5,5-dimethyl-1,3-cyclohexandione or 1,3-cyclohexandione in present heterogeneous catalysts silica-supported antimony(III)chloride (SbCl3/SiO2) and nano catalyst CdO under condition reflux in Ethanol. The advantages this method can be presented to the use of catalysts cheap, accessible, simple separation products, improve the efficiency of products, the use of solvents that are relatively less environmental pollution, an easy way to recyclability and reused catalyst. Also, in present work, (2A-3C-4P-5O-TBP) was used as a platform for dispersion and immobilization of AgNPs on the glassy carbon electrode. The functional groups at (2A-3C-4P-5O-TBP) have effective interaction with silver ions and cause to electrochemical immobilization of AgNPs on the electrode surface. The surface of electrode was investigated by scanning electron microscopy (SEM) and the results showed good distribution of AgNPs on the electrode surface modified with (2A-3C-4P-5O-TBP). | ||
| Keywords | ||
| Tetrahydrobenzo[b]pyran; Green chemistry; silica-supported antimony(III)chloride; Cadmium oxide; Silver nanoparticle; Glasy carbon electrode | ||
| References | ||
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